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Biological Magnetic Resonance Data Bank
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Instrumentation and Ionization Methods Tutorial
Ionization Methods
EI, CI
Electron ionization (EI) is widely used in mass spectrometry for relatively volatile samples that are insensitive to heat and have relatively low molecular weight. The spectra, usually containing many fragment-ion peaks, are useful for structural characterization and identification. Small impurities in the sample are easy to detect. Chemical Ionization (CI) is applied to similar samples; it is used to enhance the ...
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Better Instrumentation and Measurements through Spectrochemical Research
The Laboratory for Spectrochemistry (LFS) has several missions: 1) to develop spectrochemical measurements and instrumentation; 2) to characterize spectrochemical events and systems fundamentally through experimental measurements and theoretical modeling; 3) to solve practical problems through spectrochemical techniques; and 4) to integrate spectrochemical measurements and instrumentation with other techniques. Research in the LFS ranges from plasma physics to chemical sensors and includes both optical and mass spectrometry. Areas of application include on-site monitoring, environmental science, bioanalysis, and materials chemistry.
ALUMNI: PLEASE UPDATE YOUR INFORMATION BY CLICKING HERE
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Home > Troubleshooting
FTIR Troubleshooting
Using our vast FTIR service experience we have compiled this list of symptoms and causes for ailments common to all FTIR systems, regardless of the vendor. This list will be updated frequently. Please contact us with suggestions or inquiries.
DISCLAIMER: Many of the suggestions provided here should only be performed only by a qualified service engineer. High voltages may be present. Laser light is potentially harmful to your ...
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The Mass Spec Detector
Mass Spectral Interpretation
GC/MS Data
MS Examples
Test your knowledge.
This 'short course' is designed as an introduction to the use of a Mass Spectrometer as a GC detector. Lecture slides can be viewed by selecting a topic above. This material is copyright (C) 2004 James K. Hardy and The University of Akron. This material was last updated on .
Table of Common Fragments.
Table of Common Losses.
Please contact James K. Hardy if you have any questions or comments.
The views and opinions expressed in this page are strictly those of the page author. The contents of this page have not been reviewed or approved by The University of Akron.
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Introduction to Mass Spectrometry
An introductory tutorial for students at the University of Arizona -- contents:
INTRODUCTION: a brief description of a quadrupole instrument, information provided by an EI mass spectrum (including a table of common isotopes), a listing of other methods, and some helpful websites
EXAMPLES: characteristic fragments observed in compounds presented by functional group
INTERPRETATION: the basic steps to interpret an EI mass spectrum
QUIZZES: Each quiz listed below is designed to help you learn how to interpret EI mass spectra
AlcoholsAlkanesAminesEstersHalides
AldehydesAmidesCarboxylic acidsEthersKetones
Written by L.Breci
breci@u.arizona.edu
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Scientific Instrument Services, Inc.
Supplies and Services for Mass Spectrometers, Gas Chromatographs and Liquid Chromatographs
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Application Notes | Adsorbent Resins | MS Tips | Newsletter | MSDS | MS Tools
MS Tools
Mass Spec Tools is designed to be an information source for the mass spectrometer community. We hope that the following information, tools, and references will be of use to you. If you hav ...
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By Uwe Oehler
(Thanks to Yu Fei Cai for corrections and comments)
[To Dr. Iguana Does Chemistry]
Contents
Introductory Comments
Theory of NMR
Introductory Comments
Spin
The External Magnetic Field
Precession
Energies
Population Distribution
The NMR experiment
The NMR Spectrum
Introductory Comments
Shielding and Deshielding - Chemical Shift
Chemical Shift - Electronegativity
Chemical Shift - -System Ring Currents
Integration and Saturation
Dipolar Coupling
Second Order Coupling Effects
Relaxation and Linewidths
Quadrupolar Coupling
Interpreting the NMR Spectrum
Introductory Comments
Instrumentation
Introduction
CW Instruments
Pulse Instruments
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University of Erlangen-Nuremberg, Institute of Organic Chemistry
Auditory Presentation of Free Induction Decay (FID) Signals Generated by NMR Spectrometers
or
Copyright © 1996 Walter Bauer, Institute of Organic Chemistry,
University of Erlangen-Nuremberg, Germany
Dedicated to Prof. Dr. Dr. h. c. Dieter Seebach on the occasion of his 60th birthday
This is an article written for the WWW. To read this article, you may either go from top to bottom by clicking th ...
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Nuclear Magnetic Resonance
1/23/98
Click here to start
Table of Contents
Nuclear Magnetic Resonance
Proton NMR
Magnetic moment precess in a magnetic field
Energy Difference
Resonance
Resonance
Detection
Fourier Transform
Chemical Shift
Chemical Shift (cont.)
Tetramethylsilane
Chemical Shift (cont.)
Chemical Shift (cont.)
Electronegativity Influences Chemical Shifts
A Spectrum
Diamagnetic Anistropy
Aromatics
Some chemical shifts
Magnetic Equivalence
More
Spin-spin ...
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Scripps Center for Mass Spectrometry Home
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The information you have requested will most likely be found by navigating the links provided on the left.
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Welcome to the Society for Applied Spectroscopy
Your Portal to Spectroscopy on the Internet
Mission
The Society for Applied Spectroscopy is a nonprofit organization formed to advance and disseminate knowledge and information concerning the art and science of spectroscopy, and other allied sciences, to advance the professional standing and growth of the Society and its members, to coordinate cooperative endeavors of its individual members and sections, and to promote and ...
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The Basics of NMR is an introductory hypertext book on nuclear magnetic resonance spectroscopy. NMR spectroscopy is an instrumental technique used by scientists to determine structure and dynamical information about molecules. One of the most difficult things to comprehend about NMR is the dynamical nature of its principals. This website combines text, figures, and animations to explain NMR spectroscopy. The website has been of value to students wishing to learn about NMR, educators teaching the principals of NMR, and researchers wishing to check a quick fact about NMR. The website requires no special plugins to be viewed.
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Problems in NMR and IR Spectroscopy
Welcome to WebSpectra - This site was established to provide chemistry students with a library of spectroscopy problems. Interpretation of spectra is a technique that requires practice - this site provides 1H NMR and 13C NMR, DEPT, COSY and IR spectra of various compounds for students to interpret. Hopefully, these problems will provide a useful resource to better understand spectroscopy.
This project is supported by Cambridge Isotope Laboratories an ...
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Click Here for an Index search.
Browse through the Global Instructional Chemistry pages.
NMR Spectroscopy. Principles and Application.
Six second year lectures given at Imperial College by Henry Rzepa.
http://www.ch.ic.ac.uk/local/organic/nmr.html
Index of Lectures
Pre-amble
What Nuclear Magnetic Resonance Can Measure
Principles of Nuclear Magnetic Resonance
A Collection of Identical Protons
A Collection of Different Protons
The Situation for Other Nuclei
How to D ...
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